Nitro-Explosives: A Practical Treatise by P. Gerald Sanford
page 112 of 352 (31%)
page 112 of 352 (31%)
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| | | | | | | | From | To | Increase. | Loss. | |________________|_______|_______|___________|_______| | | | | | | | 1. Clear | 57° | 62° | 31 | ... | | 2. " | 60° | 62° | 18 | ... | | 3. Cloudy | 60° | 62° | 7 | ... | | 4. Rain | 60° | 63° | 0 | 0 | | 5. Clear | 58° | 62° | 15 | ... | | 6. Rainy | 58° | 62° | ... | 2 | | 7. Cloudy | 62° | 65° | ... | 10 | | 8. Clear | 60° | 62° | 5 | ... | | 9. Partly Clear| 50° | 60° | ... | 3 | |10. " | 58° | 60° | ... | 10 | |11. Cloudy | 58° | 60° | 8 | ... | |12. Rainy | 58° | 60° | ... | 10 | |13. Partly CLear| 50° | 58° | 20 | ... | |14. Cloudy | 50° | 60° | 16 | ... | |________________|_______|_______|___________|_______| The lesson this table teaches is, that it is almost impossible to nitrate cellulose in small quantities, and get uniform results, when the nitration is carried on at high temperatures. As regards the solubility of pyroxyline, Parks found that nitro-benzene, aniline, glacial acetic acid, and camphor, dissolved in the more volatile solvents methyl-alcohol and alcohol-ether, were much the best solvents for producing a plastic, as they are less volatile, and develop greater solvent action under the influence of heat. Nitro-benzene gives a solution that is granular; it seems to merely convert the pyroxyline, and not to dissolve it; but on the |
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