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Nitro-Explosives: A Practical Treatise by P. Gerald Sanford
page 286 of 352 (81%)

[Footnote A: Dr G. Spica (_Rivista_, Aug. 1897) proposes to use
hydrochloride of meta-phenylenediamine.]

~Exudation and Liquefaction Test for Blasting Gelatine, Gelatine Dynamite,
&c.~--A cylinder of blasting gelatine, &c., is to be cut from the
cartridge to be tested, the length of the cylinder to be equal to its
diameter, and the ends being cut flat. The cylinder is to be placed on end
on a flat surface without any wrapper, and secured by a pin passing
vertically through its centre. In this condition the cylinder is to be
exposed for 144 consecutive hours (six days and nights) to a temperature
ranging from 85° to 90° F. (inclusive), and during such exposure the
cylinder shall not diminish in height by more than one-fourth of its
original height, and the upper cut surface shall retain its flatness and
the sharpness of its edge.

~Exudation Test.~--There shall be no separation from the general mass of
the blasting gelatine or gelatine dynamite of a substance of less
consistency than the bulk of the remaining portion of the material under
any conditions of storage, transport, or use, or when the material is
subjected three times in succession to alternate freezing and thawing, or
when subjected to the liquefaction test before described.

~Picric Acid.~--The material shall contain not more than 0.3 part of
mineral or non-combustible matter in 100 parts by weight of the material
dried at 160° F. It should not contain more than a minute trace of lead.
One hundred parts of the dry material shall not contain more than 0.3 part
of total (free and combined) sulphuric acid, of which not more than 0.1
part shall be free sulphuric acid. Its melting point should be between
248° and 253° F.
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