Nitro-Explosives: A Practical Treatise by P. Gerald Sanford
page 85 of 352 (24%)
page 85 of 352 (24%)
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In carrying out this invention a rectangular lead-lined or earthenware tank _a_ is employed, having a false bottom _b_, supported by ribs _c'_, over the real bottom _c_, which slopes down to a draining outlet pipe _d_, provided with a perforated grid or plate _e_, adapted to prevent choking of the outlet. Suitably supported near the top of the vessel _a_ are provided two troughs, _f_ having depending aprons _g_, a pipe _h_ has two branches _h'_, leading to the troughs, _f_. This pipe _h_ is adapted to be connected by a rubber pipe either to the outlet pipe _k'_ of the sulphuric acid tank _k_ or the water supply pipe _l_. The nitrating acids are supplied through the pipe _m_. A charge of mixed nitrating acids is introduced into the vessel _a_ say up to the level _n_, and the dry cellulose thrown into the acids in small quantities at a time, being pushed under the surface in the usual way. [Illustration: FIG. 21.--PLAN OF THOMSON'S APPARATUS, _a_, Tank; _b_, False Bottom; _c'_, Ribs; _e_, Grid; _f_, Troughs; _g_, Aprons; _h_ and _h'_, Pipes to Troughs _f_; _k_, Sulphuric Acid Tank; _m_, Pipe to Nitrating Acids Tank; _o_, Perforations of Troughs; _p_, Cock to remove Acid.] A thin layer, say half an inch, of a suitable liquid, preferably sulphuric acid, of a gravity not exceeding that of the waste acid to be produced, is run carefully on the top of the acids by means of the troughs _f_, which are perforated as shown at _o_, so that the sulphuric acid runs down the aprons _g_, and floats on the nitrating acids. The whole is then allowed to stand till nitration has been completed. Water is then supplied to the troughs by way of the pipes _l_, _h_, and _h'_, and is allowed to float very gently over the surface of the sulphuric acid, and when a sufficient layer has been formed, the cock _p_ at the bottom of the apparatus is |
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