Nitro-Explosives: A Practical Treatise by P. Gerald Sanford
page 108 of 352 (30%)
page 108 of 352 (30%)
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[Illustration: FIG. 23.--VESSEL FOR NITRATING COTTON OR PAPER.]
The nitrating apparatus of White and Schupphaus (U.S.P., No. 418, 237, 89) Mr Field considers to be both novel and excellent. The cage (Fig. 24), with its central perforated cylinder (Fig. 25), is intended to ensure the rapid and perfect saturation of the tissue paper used for nitrating. The patentees say that no stirring is required with their apparatus. This, says Mr Field, might be true when paper is used, or even cotton, when the temperature of nitration is from 30° to 35° C., but would not be true if the temperature were raised to 50° to 55° C. The process is as follows:-- The paper is nitrated in the cage (Fig. 25), the bottom of which is formed by the flanged plate C, fastened to the bottom of the internal cylinder B. After nitration the cage is carried to a wringer, which forms the basket, and the acids removed. Finally, the cage is taken to a plunge tank, where the paper is removed from the cage by simply pulling out the central perforated cylinder B. Fig. 26 shows the nitrating pot, with its automatic cover. The plunge tank is shown in plan and section in Figs. 28 and 29. This apparatus is suitable for the nitration of cotton fibre in bulk at high or low temperatures. Other methods that have been patented are Mowbray's (U.S.P., No. 434, 287), in which it is proposed to nitrate paper in continuous lengths, and Hyatt's (U.S.P., No. 210, 611). [Illustration: FIG. 24.--CENTRAL PERFORATED CYLINDER.] [Illustration: FIG. 25.--THE CAGE. WHITE AND SCHUPPHAUS' NITRATING APPARATUS.] [Illustration: FIG. 26.--CELLULOID NITRATING POT.] [Illustration: FIG. 27.--ANOTHER VIEW.] |
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